127956-11-0, Methyl 4-oxotetrahydro-2H-pyran-3-carboxylate is a Tetrahydropyrans compound, ?involved in a variety of chemical synthesis. Rlated chemical reaction is continuously updated
Oxotetrahydro-2H-pyran-3-carboxylate (1 g, 6.3 mmol)Was dissolved in acetonitrile (50 mL) and thiourea (722 mg, 9.5 mmol) and DBU (1.15 g, 7.6 mmol) were added,85 C for 2 hours. The reaction was completed, cooled to room temperature, evaporated to dryness solvent, 20mL of water was added, the pH was adjusted to acidic with concentrated hydrochloric acid, precipitated solid, filtered and the filter cake was dried to give 900mg, yield: 77.6%., 127956-11-0
The synthetic route of 127956-11-0 has been constantly updated, and we look forward to future research findings.
Reference£º
Patent; Shandong Xuanzhu Pharmaceutical Technology Co., Ltd.; Wu Yongqian; Qi Qu; Zu Chao; (36 pag.)CN107226808; (2017); A;,
Tetrahydropyran – Wikipedia
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